气泡在超声场中绕圈运动的高速摄影及其图像分析

借助高速摄影和图像分析技术对首次发现的附壁气泡的绕圈现象进行了实验研究,重点研究游移气泡的运动轨迹、附壁气泡的布阵过程、气泡的来源以及气泡的振动细节.研究发现游移绕圈气泡的运动轨迹呈现出不稳定、不规则、不光滑的特点.阵列气泡源于游移气泡,而游移气泡变成阵列气泡的方式主要是通过合并增大体积,从而减小所受的Bjerknes力,降低活性的方式实现的.游移气泡源于ALF(acoustic lichtenberg figure)空化云中大量空泡的合并,使以径向振动为主的空泡逐渐过渡到以表面波动为主的气泡.阵列气泡在Bjerknes力的作用下呈现出规则的表面波动,而体积更小受力更大的游移空泡的表面完全失稳,呈现极不规则的形貌,并对附近阵列气泡的表面波动产生影响.阵列气泡呈现出十分规则的排布,相邻阵列气泡之间的振动相位是相反的,表现为相互排斥.     

Experimental Study of Effect of Temperature Variations on the Impedance Signature of PZT Sensors for Fatigue Crack Detection

Structural health monitoring (SHM) is recognized as an efficient tool to interpret the reliability of a wide variety of infrastructures. To identify the structural abnormality by utilizing the electromechanical coupling property of piezoelectric transducers, the electromechanical impedance (EMI) approach is preferred. However, in real-time SHM applications, the monitored structure is exposed to several varying environmental and operating conditions (EOCs). The previous study has recognized the temperature variations as one of the serious EOCs that affect the optimal performance of the damage inspection process. In this framework, an experimental setup is developed in current research to identify the presence of fatigue crack in stainless steel (304) beam using EMI approach and estimate the effect of temperature variations on the electrical impedance of the piezoelectric sensors. A regular series of experiments are executed in a controlled temperature environment (25°C–160°C) using 202 V1 Constant Temperature Drying Oven Chamber (Q/TBXR20-2005). It has been observed that the dielectric constant ε₃₃^T which is recognized as the temperature-dependent constant of PZT sensor has sufficiently influenced the electrical impedance signature. Moreover, the effective frequency shift (EFS) approach is optimized in term of significant temperature compensation for the current impedance signature of PZT sensor relative to the reference signature at the extended frequency bandwidth of the developed measurement system with better outcomes as compared to the previous literature work. Hence, the current study also deals efficiently with the critical issue of the width of the frequency band for temperature compensation based on the frequency shift in SHM. The results of the experimental study demonstrate that the proposed methodology is qualified for the damage inspection in real-time monitoring applications under the temperature variations. It is capable to exclude one of the major reasons of false fault diagnosis by compensating the consequence of elevated temperature at extended frequency bandwidth in SHM.     

SH wave propagation in a piezoelectric/piezomagnetic plate with an imperfect magnetoelectroelastic interface

In this paper, we investigate the SH wave propagation in a layered piezoelectric (PE) and piezomagnetic (PM) plate with an imperfect magnetoelectroelastic interface. A linear magnetoelectroelastic spring model is used to describe the weakness of the imperfect interface. On the basis of this model, dispersion curves and mode shapes of the SH waves are computed. In particular, a PZT-5A/CoFe₂O₄ composite plate is considered in the numerical examples to calculate the dispersion curves and the mode shapes for different combinations of the magnetic, electrical and elastic spring constants. The effects of the layer thickness ratio and the electric-magnetic boundary conditions on the dispersion curves are discussed in details. Our results show that for a general weak bonding case, the high modes of the dispersion curves are not monotonous in the range of small wave numbers. With the layer thickness ratio increasing, the wave velocities of the SH waves increase. The electric boundary conditions mainly determine the dispersion curves of the SH waves in the case of a small layer thickness ratio, i.e. a large thickness of the PE layer. The present results have relevant applications in the nondestructive testing and evaluation of the layered PE/PM plate-like wave devices.     

Zinc‐containing ionic liquid as a dual solvent‐catalyst in base‐free condensations under ultrasonic irradiation

In this study, natural‐based ionic liquid (IL) using caffeine (Caff), trietahnolamine (TEA) and ZnBr₂, [Caff‐TEA]⁺[ZnBr₃]^?, which features high catalytic activity and environmentally‐friendly nature was synthesized with melting point of 76 °C by a facile method. The synthesized [Caff‐TEA]⁺[ZnBr₃]^? has high catalytic activity as both of catalyst and solvent in condensation reactions for the synthesis of benzylidenes, bis‐hydroxyenones and xanthenes. Synthesized IL was characterized by proton nuclear magnetic resonance (¹HNMR), Fourier transform infrared spectroscopy (FT‐IR), X‐ray diffraction (XRD) and Energy‐dispersive X‐ray spectroscopy (EDX) analysis. Also synthesized heterocycles were characterized by FT‐IR, proton nuclear magnetic resonance (¹HNMR) and carbon nuclear magnetic resonance (¹³CNMR).     

含非完整界面的功能梯度压电材料Ⅲ型裂纹问题

本文研究了含非完整界面的功能梯度压电复合材料的Ⅲ型裂纹问题．此裂纹垂直于非完整界面，采用弹簧型力电耦合界面模型模拟非完整界面．界面两侧材料的性质，如弹性模量、压电常数和介电常数均假定呈指数函数形式且沿着裂纹方向变化．运用积分变换法将裂纹面条件转换为奇异积分方程，并使用Gauss-Chebyshev方法对其进行数值求解．根据算例结果讨论了一些退化问题并分析了裂纹尖端强度因子与材料的非均匀系数和非完整界面参数的关系．     

主动控制压电旋转悬臂梁的参数振动稳定性分析

在工程实际中旋转机械由于制造和加工误差,装配的不均匀性等原因,往往会脉动运行,这将使得机械系统发生参数振动. 当脉动参数满足一定关系时,这种参数振动将会失稳,进而影响机械结构的正常运转. 本文针对这一问题,引入压电材料对 脉动旋转悬臂梁系统的振动进行控制,研究主动控制悬臂梁系统的参数振动优化设计问题,采用 Hamilton 变分原理与一阶 Galerkin 离散相结合的方法,建立了受速度反馈传感器主动控制的压电旋转悬臂梁的一阶近似线性控制方程. 运用多尺度方法,得到了压电旋转悬臂梁系统在发生1/2亚谐波参数共振时稳定性边界的控制方程,并利用直接分析方法验证了解析摄动解的正确性. 将摄动解中临界阻尼比和轮毂角速度脉动幅值的无量纲参数作为评价系统稳定性能的指标. 通过数值算例,分析了轮毂半径、轮毂角速度平均值和脉动幅值、梁长以及速度传感器的反馈增益系数对系统稳定性区域的影响. 研究结果表明,梁长、轮毂半径、脉动幅值会降低系统稳定性,反馈增益系数可以提高系统稳定性,而轮毂角速度平均值与系统稳定性之间有非单调的关系. 为进一步设计压电旋转机械结构提供了理论依据.      

A facile approach to prepare water-soluble magnetic metal (oxide) frameworks based on Na,Ca alginate and maghemite

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超声波燃气表矩形流道的雷诺修正系数仿真研究

在超声波流量计测量技术中, 雷诺修正系数相关的研究对于提高计量精度有重要作用. 为研究矩形流道的雷诺修正系数与雷诺数的关系, 对矩形流道在常温常压流量较小情况下进行仿真, 结果发现: 矩形流道层流状态下的雷诺修正系数与雷诺数呈线性相关. 保持压强、体积流量不变, 在不同温度下进行仿真及拟合, 结果表明: 在不同温度下雷诺修正系数与雷诺数的线性关系依然满足. 在上述实验基础上, 对矩形流道湍流状态下的雷诺修正系数与雷诺数关系进行研究, 通过改变温度、压强和体积流量进行仿真及拟合发现, 矩形流道湍流状态下雷诺修正系数与雷诺数呈非线性相关.     

压电式微滴按需喷射的过程控制和规律

微滴喷射增材制造技术中沉积微滴的大小与均匀性是影响成型件质量的关键因素.本文设计了一种用于生成均匀微滴的压电驱动式微滴喷射装置,通过压电材料带动柔性膜片振动,将液体从喷嘴中喷出生成微滴,采用数值模拟和实验相结合的方法,研究了不同控制参数下膜片振幅及其对生成微滴尺寸和均匀性的影响.研究结果表明:膜片振幅大小受到驱动电压和压电频率的共同影响,压电频率是导致膜片中心点振幅实验测量值小于理论计算值的主要原因,膜片振动会导致喷嘴内部压力发生变化从而影响微滴生成尺寸.在相同驱动电压条件下,压电频率为10 Hz时存在压电膜片振幅最大值.随着膜片振幅的增大,喷孔处液体速度和液柱长度增大到临界值时可以生成微滴,当喷孔处的液柱长度超过临界值时,会形成卫星液滴. 当膜片振幅区间在30 $\mu$m$\sim $42 $\mu $m可以稳定生成微滴,生成最小微滴尺寸为339.8$\mu$m,直径最大变化率为0.29%,相邻两微滴间距最大变化率为2.67%,生成微滴的尺寸及均匀性较好.研究结果有助于提高压电式微滴喷射装置的液滴生成质量.      

Solvent selection in ultrasonic-assisted emulsification microextraction: Comparison between high- and low-density solvents by means of novel type of extraction vessel

There are numerous published reports about dispersive liquid phase microextraction of the wide range of substances, however, till now no broadly accepted systematic and purpose oriented selection of extraction solvent has been proposed. Most works deal with the optimization of available solvents without adequate pre-consideration of properness. In this study, it is tried to compare the performances of low- and high-density solvents at the same conditions by means of novel type of extraction vessel with head and bottom conical shape. Extraction efficiencies of seven basic pharmaceutical compounds using eighteen common organic solvents were studied in this work. It was much easier to work with high-density solvents and they mostly showed better performances. This work shows that although exact predicting the performance of the solvents is multifaceted case but the pre-consideration of initial selection of solvents with attention to the physiochemical properties of the desired analytes is feasible and promising. Finally, the practicality of the method for extraction from urine and plasma samples was investigated.